SOFT X-RAY MICROCHARACTERIZATION BEAMLINE

Microprobe Endstation

  Available

The microprobe endstation operates under vacuum and is specifically tailored for applications requiring the challenging medium-energy range of 2-4 keV. This endstation utilizes a pair of Kirkpatrick-Baez (K-B) mirrors to focus the collimated beam to a spot size of 10 µm × 10 µm for mapping experiments. A high-resolution and large-area CCD camera is equipped to obtain an optical image of the sample. Micro-XAS can also be performed on specific spots using the microprobe.

Capabilities

  • Vacuum compatible
  • 20 cm long mirror
  • 0.15 × 0.15 mrad²
  • 10 × 10 µm² beam
  • C/Pt bi-layer coating
  • 30 cm working distance
  • 7-element Si drift detector
  • mapping in fluorescence and TEY mode
  • micro-XANES

Samples

  • Thin layer
  • Films
  • Powders
  • Potential application: imaging of geological and biological samples at ~10 µm

Schematic

microprobe_schematic.png

Specifications

Source Bending Magnet
Energy Range (keV) 1.7 - 10
Wavelength (Å) 7.3 - 1.3
Resolution ΔE/E @ E InSb (111) 3.3 × 10⁻⁴
Resolution ΔE/E @ E Si (111) 1.0 × 10⁻⁴
Flux (g/s/0.1%BW) @ 100 mA 1.0 × 10⁹
Spot Size (V × H) ~10 µm × 10 µm
Focusing K-B Mirror Pair

microprobejpeg.jpg

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